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Basic Corrosion Package 기본 부식실험용 패키지

  • 장비 및 부식 실험용 cell kit, 부식 연구에 대한 핸드북 제공

· 첨부파일

Basic Corrosion Package에 제공되는 EmStat4S HR Potentiostat/Galvanostat 연구  실험용으로 크기가 작은 (7.2 x 5.5 x 2.6 cm3) 휴대형 potentiostat입니다
부식 속도를 결정하기 위해 최대 200 mA까지 사용할  있는 광범위한 전류 범위를 가지고 있으며 부식 분석에 사용되는 모든 일반적인 전기화학 테크닉을 제공합니다
Potentiostatic Polarization, Linear Polarization, Cyclic Polarization, Corrosion Potential 
측정 뿐만 아니라 Potentiostatic, Open Circuit Potential(EOC) 측정합니다.

 장비는 자동 또는 수동 분석을 위한 다양한 부식 분석 테크닉을 지원하는 PSTrace5 소프트웨어와 함께 제공됩니다.

EmStat4S HR 패키지(Standard) :

  • Corrosion Cell
  • Corrosion Handbook
  • EmStat4S HR (C-ES4S-HR.F0)
  • 장비 휴대용 케이스
  • 2mm 바나나 커넥터가 달려 있는 고품질의 이중 차폐  케이블
  • 악어 클립
  • USB 케이블
  • PSTrace 소프트웨어

Techniques

EmStat4S HR Potentiostat/Galvanostat에서 지원되는 테크닉은 다음과 같습니다.

Corrosion techniques :

  • Potentiostatic Polarization
  • Galvanostatic Polarization
  • Linear Polarization
  • Cyclic Polarization
  • Corrosion Potential
  • Zero Resistance Ammeter (ZRA)

Voltammetric techniques :

  • Linear Polarization
  • Cyclic Polarization
  • Differential pulse voltammetry (DPV)
  • Square wave voltammetry (SWV)
  • Normal pulse voltammetry (NPV)
  • AC Voltammetry (ACV)* (2021/11월 업데이트 예정)
  • Stripping chronopotentiometry (PSA or SCP) (stripping mode에서 사용)

Techniques as a function of time :

  • Corrosion Potential Measurement
  • Chronoamperometry (CA)
  • Pulsed amperometric detection (PAD)
  • Multiple pulse amperometry (MPAD)* (2021/11월 업데이트 예정)
  • Fast amperometry (FAM)* (2021/11월 업데이트 예정)
  • Chronopotentiometry (CP)
  • Multistep amperometry (MA)
  • Open circuit potentiometry (OCP)
  • Multistep Potentiometry (MP)
  • Mixed Mode (MM)* (2021/11월 업데이트 예정)

Specifications

C-ES4S-HR.F0 사양

일반

Potential range

± 6 V

Max. compliance voltage

± 8 V

Current ranges

100 nA to 100 mA (7 ranges)

Max. current

± 200 mA

 

Potentiostat

applied potential resolution

183 μV

applied potential accuracy

≤ 0.2% ±1 mV offset

current ranges

100 nA to 100 mA (7 ranges))

measured current resolution

0.009% of CR (92 fA on 1 nA range)

measured current accuracy

≤ 0.2% at Full Scale Range

 

Galvanostat

current ranges

1 uA, 100 uA, 10 mA, 100 mA (4 ranges)

applied dc-current

±3 * CR (current range)

applied dc-current resolution

0.0183% of CR)

applied dc-current accuracy

<0.4% (gain) + 0.002 * CR (offset)

measured dc-potential resolution

193 μV (gain 1)
96.5 μV (gain 2)
38.5 μV (gain 5)
19.3 μV (gain 10)
9.65 μV (gain 20)

measured dc-potential accuracy

≤ 0.2% ±1 mV offset

 

Electrometer

electrometer amplifier input

 > > 1 TΩ // 10 pF

bandwidth

10 kHz default or 500 kHz for EIS and fast CA/CP

 

 

 Software

http://www.palmsens.co.kr/img/PSTrace5_overview.png

Corrosion Mode

PSTrace5 소프트웨어에는 부식 테크닉을 지원하는 Corrosion mode가 있습니다. 

  • Tafel analysis
  • Determine Corrosion Potential and Current
  • Circuit fitting
  • Determine Corrosion Rate 

http://www.palmsens.co.kr/img/TafelSmall.gif

PSTrace5 소프트웨어는 Equivalent Circuit Fitting 기능을 지원합니다. 

http://www.palmsens.co.kr/img/pstrace_fitting_hq_small.gif

 

 Corrosion Cell

http://www.palmsens.co.kr/img/IS-CCS-Corrosion-Cell-Set.jpg

 셀은 일반적인 부식 관련 측정에 적합한 셀로 부식  세트에는 다음이 포함되어 있습니다 :

  • 2*Counter Electrode
  • 2*Counter Electrode
  • 1*PTFE ring
  • 2*ThreadedAdapter for T24/40 Joint
  • 1*Reference Electrode
  • 1*Reference Electrode Bridge Tube
  • 5*Reference electrode bridge core
  • 1*Purge Tube
  • 1*Electrode Mounting Rod
  • 1*Screw nut
  • 1*PTFE pad
  • 1*Working Electrode Hoder
  • 5*Replacement Teflon Gaskets
  • 1*Working Electrode tip
  • 1*1000ml Corrosion Flask
  • 1*Ball clip
  • 1*Flat Specimen Holder Kit